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离线纯化水TOC水质分析仪

离线纯化水TOC水质分析仪

价格:38450元浏览:70次联系:刘元元 / 15132636097 / 企业:北京北广精仪仪器设备有限公司留言店铺收藏

离线纯化水TOC水质分析仪  产品特点

1.仪器采用便携设计,使用轻便,方便移动至取样点。

2.采用嵌入式系统,触摸屏设计,纯中文操作方便简易。

3.针对制药用水(TOC含量在1000ppb以下)总有机碳含量的检测设计,进行检测。

4.配备大量的储存空间,能够存储大量的测试数据。

5.中文打印,输出测试参数、测试结果。

6.在使用、贮存和更换过程中不需要气体或试剂,无移动部件,减少维修和维护成本。

7.当测试样品浓度超过规定限度,仪器能够自动报警,并输出控制信号。

8.符合国家《中国药典》 CP2010规定的测试方案,可以提供IQ/OQ/PQ服务。

离线纯化水TOC水质分析仪  氧化反应器

仪器利用UV射线在二氧化钛光催化剂的作用下将有机化合物氧化成二氧化碳,氧化反应器是一个UV灯外包螺旋形的石英管。UV灯发出185nm和254nm的光线,使水产生光分解。

H2O hν(185nm)(TiO2)? OH?  H?

羟基自由基(OH?)能完全把有机化合物氧化为二氧化碳。

有机物  OH?? CO2 H2O

UV灯的使用寿命为6个月,当更换时间到期时仪器将出现警告信息,提醒用户更换UV灯。

二氧化碳测量循环

仪器每4分钟检测得出一个数据(包括TOC值和电导率值),在4分钟的测量循环中TC和TIC是独立检测的。

装箱清单

 

试验主机

一台

采集管

两条

电源线

一条

控制系统

一套

数据采集系统

一套

产品使用说明书

一份

产品合格证、保修卡

一份

 

测定原理:仪器采用紫外氧化的原理,将水溶液中的总有机碳氧化为二氧化碳,并且测定其含量,二氧化碳的测试采用的是直接电导率法,通过测试经过氧化反应的水溶液总碳含量和未经过氧化反应的样品总无机碳的含量差值来测定总有机碳含量,即:总有机碳(TOC)=总碳(TC)-总无机碳(TIC)。

TOC就是关于进行改进和如何最好的实施这些改进的一套管理理念和管理原则,可以帮助企业识别出在实现目标的过程中存在着哪些制约因素——TOC称之为“约束”,并进一步指出如何实施必要的改进来一一消除这些约束,从而更有效的实现企业目标。

Product Features

1. The instrument adopts a portable design, which is easy to use and convenient to move to the sampling point.

2. Adopting an embedded system and touch screen design, pure Chinese operation is convenient and easy.

3. Design and conduct testing for the total organic carbon content of pharmaceutical water (TOC content below 1000ppb).

4. Equipped with a large amount of storage space, capable of storing a large amount of test data.

5. Print in Chinese and output test parameters and results.

6. No gas or reagents are required during use, storage, and replacement, and there are no moving parts, reducing maintenance and repair costs.

When the concentration of the test sample exceeds the specified limit, the instrument can automatically sound an alarm and output a control signal.

8. According to the testing plan specified in the Chinese Pharmacopoeia CP2010, IQ/OQ/PQ services can be provided.

Oxidation reactor

The instrument uses UV rays to oxidize organic compounds into carbon dioxide under the action of titanium dioxide photocatalyst. The oxidation reactor is a spiral quartz tube wrapped around a UV lamp. The UV lamp emits light at 185nm and 254nm to decompose aquatic products.

H2O hν(185nm)(TiO2)OH? H?

Hydroxyl radicals (OH?) can completely oxidize organic compounds to carbon dioxide.

Organic compounds OH?CO2 H2O

The service life of UV lamps is 6 months. When the replacement time expires, the instrument will display a warning message to remind the user to replace the UV lamp.

Carbon dioxide measurement cycle

The instrument detects data (including TOC and conductivity values) every 4 minutes, and TC and TIC are independently detected during the 4-minute measurement cycle.

Packing List

 

One experimental host

Two collection tubes

One power cord

One set of control system

A set of data collection system

One copy of the product user manual

One copy of product qualification certificate and warranty card

 

Measurement principle: The instrument adopts the principle of ultraviolet oxidation to oxidize the total organic carbon in the aqueous solution to carbon dioxide and determine its content. The carbon dioxide test adopts the direct conductivity method, which determines the total organic carbon content by testing the difference between the total carbon content of the oxidized aqueous solution and the total inorganic carbon content of the sample without oxidation reaction, that is, total organic carbon (TOC)=total carbon (TC) - total inorganic carbon (TIC).

TOC is a set of management concepts and principles about making improvements and how to best implement them. It can help companies identify the constraints that exist in the process of achieving their goals, which TOC refers to as "constraints", and further point out how to implement necessary improvements to eliminate these constraints one by one, in order to more effectively achieve their corporate goals.

 

废水的性质或水质是水和各种杂质组成的复杂体系所表现出来的综合特性,这种特性在工程实...急性毒性的单位通常是以在特定暴露时间内使试验生物死亡50%的毒物或废水浓度,即半致死浓度LD50来表示。

 

从理论上对化工污水TOC与COD_a的相关性进行了分析,对在实际工作中测得的TOC和COD_a数据进行了回归分析。结果表明,化工污水的TOC和COD_a之间有着良好的相关性。在一定条件下,利用回归方程可以从测得的TOC值推算出COD_a值,或者从COD_a值推算出TOC值。因此,TOC值可以用来表示有机废水的污染程度,也可做为有机污染物的一个控制指标。

 

有很好的相关性[Z,31一、前言在同一废水样中,如无其它干扰,且氧化完全,则测得的TOC值与COD值成正比例关系,长期以来,评价水体中有机物朽染的程度即COD—KTOC。因C Oz—CO卜所以*一都是利用经典方法测定COD和BOD。BOD/五32/12=2.667。

 应用范围

该仪器可用于检测制药工业中纯化水、注射用水和去离子水中有机碳的浓度;也可用于半导体行业中超纯水TOC的检测。

在制药领域和生物化学领域清洁验证过程中,可用于验证清洁效果。

该仪器具有在线检测功能,可以在线监测制药工业的制水系统、半导体工业的超纯水制备系统和晶片工艺过程、电厂去离子水制备过程等。

 离线检测

离线检测时,仪器可从样品瓶或其它没有压力的容器直接取样。仪器管路冲洗和仪器校准应在离线状态操作。若样品中有不可溶性微粒,应经过滤膜(孔径60μm或更小)过滤后进入仪器,以防止样品中的微粒阻塞仪器。仪器的进样管为1/16英寸的Teflon管,经蠕动泵抽进管路中的水样流速约为0.5 ml/min。

主要技术参数

电   源:220V?22V

电源频率:50Hz?1Hz

额定功率:100W

基本尺寸:44cm?18cm?26cm

检测极限:0.001mg/L

检测精度:?5%

检测范围:0.001mg/L~1.000mg/L

分析时间:4min

响应时间:15 min以内

样品温度:1-95℃

环境温度:10-40℃    温度变化在?5℃/d以内

内部样品流速:0.5 ml/min

相对湿度:≤ 85%

重复性误差:≤ 3%

零点漂移:?5%

量程漂移:?5%

The nature or quality of wastewater is a comprehensive characteristic exhibited by a complex system composed of water and various impurities, which is important in engineering practice The unit of acute toxicity is usually expressed as the half lethal concentration (LD50) of the toxic substance or wastewater that causes 50% death of the test organism within a specific exposure time.

 

Theoretical analysis was conducted on the correlation between TOC and COD_a in chemical wastewater, and regression analysis was performed on the TOC and COD_a data measured in practical work. The results indicate a good correlation between TOC and COD_a in chemical wastewater. Under certain conditions, the COD_a value can be calculated from the measured TOC value using regression equations, or the TOC value can be calculated from the COD_a value. Therefore, TOC value can be used to indicate the degree of pollution in organic wastewater and can also be used as a control indicator for organic pollutants.

 

There is a good correlation [Z, 31]. Preface: In the same wastewater sample, if there is no other interference and the oxidation is complete, the measured TOC value is directly proportional to the COD value. For a long time, the degree of organic matter decay in water bodies has been evaluated as COD-KTOC. Since C Oz-CO is calculated, the classic methods are used to determine COD and BOD. BOD/5-32/12=2.667.

Application scope

This instrument can be used to detect the concentration of organic carbon in purified water, injection water, and deionized water in the pharmaceutical industry; It can also be used for the detection of TOC in ultrapure water in the semiconductor industry.

In the pharmaceutical and biochemical fields, it can be used to verify the cleaning effect during the cleaning validation process.

This instrument has online detection function, which can monitor the water production system in the pharmaceutical industry, the ultrapure water preparation system and chip process in the semiconductor industry, and the deionized water preparation process in power plants online.

Offline detection

When conducting offline testing, the instrument can directly sample from sample bottles or other containers without pressure. Instrument pipeline flushing and instrument calibration should be operated offline. If there are insoluble particles in the sample, they should be filtered through a filter membrane (with a pore size of 60μm or smaller) before entering the instrument to prevent particles from blocking the instrument. The injection tube of the instrument is a 1/16 inch Teflon tube, and the flow rate of the water sample drawn into the pipeline by a peristaltic pump is about 0.5 ml/min.

Main technical parameters

Power supply: 220V?22V

Power frequency: 50Hz?1Hz

Rated power: 100W

Basic dimensions: 44cm?18cm?26cm

Detection limit: 0.001mg/L

Detection accuracy:?5%

Detection range: 0.001mg/L to 1.000mg/L

Analysis time: 4 minutes

Response time: within 15 minutes

Sample temperature: 1-95℃

Environmental temperature: 10-40℃Temperature variation within?5℃/d

Internal sample flow rate: 0.5 ml/min

Relative humidity:≤85%

Repetitive error:≤3%

Zero drift:?5%

Range drift:?5%

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